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Information card for entry 7114583
Preview
Coordinates | 7114583.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22.5 H23 Cl Fe2 N O5 P Se2 |
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Calculated formula | C22.5 H23 Cl Fe2 N O5 P Se2 |
Title of publication | Synthesis of spiro[isoquinolinone-4,2'-oxiranes] and isoindolinones via a multicomponent reaction of 2-acetyl-oxirane-2-carboxamides, arylaldehydes and malononitrile |
Authors of publication | Bing Liu; Enxiang Wei; Shaoxia Lin; Baozhong Zhao; Fushun Liang |
Journal of publication | Chem.Commun. |
Year of publication | 2014 |
Journal volume | 50 |
Pages of publication | 6995 |
a | 9.604 ± 0.0016 Å |
b | 10.461 ± 0.0017 Å |
c | 13.63 ± 0.0019 Å |
α | 92.552 ± 0.014° |
β | 103.678 ± 0.017° |
γ | 91.248 ± 0.008° |
Cell volume | 1328.5 ± 0.4 Å3 |
Cell temperature | 113 ± 2 K |
Ambient diffraction temperature | 113 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0754 |
Residual factor for significantly intense reflections | 0.0698 |
Weighted residual factors for significantly intense reflections | 0.1679 |
Weighted residual factors for all reflections included in the refinement | 0.1792 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.056 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7114583.html
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