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Information card for entry 7114591
Preview
Coordinates | 7114591.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C66 H86 N4 Ni2 O0.5 P4 |
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Calculated formula | C66 H86 N4 Ni2 O0.5 P4 |
Title of publication | Selective P4 activation by an organometallic nickel(I) radical: formation of a dinuclear nickel(II) tetraphosphide and related di- and trichalcogenides |
Authors of publication | Stefan Pelties; Dirk Herrmann; Bas de Bruin; Frantisek Hartl; Robert Wolf |
Journal of publication | Chem.Commun. |
Year of publication | 2014 |
Journal volume | 50 |
Pages of publication | 7014 |
a | 13.7371 ± 0.0002 Å |
b | 23.694 ± 0.0005 Å |
c | 19.4754 ± 0.0003 Å |
α | 90° |
β | 91.093 ± 0.002° |
γ | 90° |
Cell volume | 6337.83 ± 0.19 Å3 |
Cell temperature | 123.01 ± 0.1 K |
Ambient diffraction temperature | 123.01 ± 0.1 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0465 |
Residual factor for significantly intense reflections | 0.0366 |
Weighted residual factors for significantly intense reflections | 0.0925 |
Weighted residual factors for all reflections included in the refinement | 0.0995 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.017 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7114591.html
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