Crystallography Open Database

Information card for entry 7114666

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Coordinates	7114666.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C58 H48 Cl F3 P4 Ru
Calculated formula	C56 H48 Cl F3 P4.5 Ru
Title of publication	A new binuclear ruthenium complex with an annelated C7 bridge via an unprecedented [2 + 2] coupling reaction
Authors of publication	Rigaut, Stéphane; Le Pichon, Luc; Touchard, Daniel; Dixneuf, Pierre H.; Daran, Jean-Claude
Journal of publication	Chemical Communications
Year of publication	2001
Journal issue	13
Pages of publication	1206
a	9.7811 ± 0.001 Å
b	12.1069 ± 0.0014 Å
c	20.503 ± 0.002 Å
α	95.204 ± 0.013°
β	98.91 ± 0.012°
γ	101.264 ± 0.013°
Cell volume	2334 ± 0.5 Å³
Cell temperature	180 ± 2 K
Ambient diffraction temperature	180 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0432
Residual factor for significantly intense reflections	0.0303
Weighted residual factors for significantly intense reflections	0.0723
Weighted residual factors for all reflections included in the refinement	0.0766
Goodness-of-fit parameter for all reflections included in the refinement	0.958
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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