Information card for entry 7114681

Structure parameters

• Formula: C43 H63 Cl4 Mo2 N7 Si4
• Calculated formula: C43 H63 Cl4 Mo2 N7 Si4
• Title of publication: Unusual molybdenum mediated C‒N bond activation
• Authors of publication: Cameron, Thomas M.; Abboud, Khalil A.; Boncella, James M.
• Journal of publication: Chemical Communications
• Year of publication: 2001
• Journal issue: 13
• Pages of publication: 1224
• a: 14.4655 ± 0.0008 Å
• b: 23.572 ± 0.001 Å
• c: 15.9891 ± 0.0009 Å
• α: 90°
• β: 104.39 ± 0.001°
• γ: 90°
• Cell volume: 5280.9 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0688
• Residual factor for significantly intense reflections: 0.0384
• Weighted residual factors for significantly intense reflections: 0.0824
• Weighted residual factors for all reflections included in the refinement: 0.093
• Goodness-of-fit parameter for all reflections included in the refinement: 0.99
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No