Information card for entry 7114684

Structure parameters

• Formula: C37 H31 Cl Ir N2 P Si
• Calculated formula: C37 H30 Cl Ir N2 P Si
• Title of publication: Iridium(iii) complexes of the new tridentate bis(8-quinolyl)silyl (‘NSiN’) ligand
• Authors of publication: Stradiotto, Mark; Fujdala, Kyle L.; Tilley, T. Don
• Journal of publication: Chemical Communications
• Year of publication: 2001
• Journal issue: 13
• Pages of publication: 1200
• a: 10.117 ± 0.0004 Å
• b: 18.08 ± 0.0006 Å
• c: 17.9962 ± 0.0004 Å
• α: 90°
• β: 104.309 ± 0.002°
• γ: 90°
• Cell volume: 3189.66 ± 0.18 ų
• Cell temperature: 149 ± 2 K
• Ambient diffraction temperature: 149 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0704
• Residual factor for significantly intense reflections: 0.0445
• Weighted residual factors for all reflections: 0.1217
• Weighted residual factors for significantly intense reflections: 0.105
• Goodness-of-fit parameter for all reflections: 1.053
• Goodness-of-fit parameter for significantly intense reflections: 1.129
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No