Information card for entry 7114785

Structure parameters

• Formula: C22 H31 N3 S Si2 W
• Calculated formula: C22 H31 N3 S Si2 W
• Title of publication: Carbon‒sulfur bond activation of thiophenes by [W(NPh){o-(Me3SiN)2C6H4}(pyridine)2]
• Authors of publication: Mills, R. C.; Abboud, K. A.; Boncella, J. M.
• Journal of publication: Chemical Communications
• Year of publication: 2001
• Journal issue: 16
• Pages of publication: 1506
• a: 9.4647 ± 0.0004 Å
• b: 11.7141 ± 0.0005 Å
• c: 12.483 ± 0.0005 Å
• α: 101.246 ± 0.001°
• β: 111.655 ± 0.001°
• γ: 93.904 ± 0.001°
• Cell volume: 1246.64 ± 0.09 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0305
• Residual factor for significantly intense reflections: 0.0264
• Weighted residual factors for significantly intense reflections: 0.0647
• Weighted residual factors for all reflections included in the refinement: 0.0663
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No