Information card for entry 7114848

Structure parameters

• Formula: C34.5 H55 N3 Si3 Tl2
• Calculated formula: C34.5 H54 N3 Si3 Tl2
• Title of publication: First structural characterization of a mixed valent thallium(i/iii) amide bearing an n-butylthallium(iii) unit stabilized by a tripodal amido ligand
• Authors of publication: Galka, Christian H.; Gade, Lutz H.
• Journal of publication: Chemical Communications
• Year of publication: 2001
• Journal issue: 10
• Pages of publication: 899
• a: 21.346 ± 0.006 Å
• b: 14.4015 ± 0.0013 Å
• c: 26.384 ± 0.01 Å
• α: 90°
• β: 107.869 ± 0.014°
• γ: 90°
• Cell volume: 7720 ± 4 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0693
• Residual factor for significantly intense reflections: 0.0471
• Weighted residual factors for significantly intense reflections: 0.1108
• Weighted residual factors for all reflections included in the refinement: 0.1287
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No