Information card for entry 7114851

Structure parameters

• Formula: C24 H26 Cu2 Mo5 N6 O27 P2
• Calculated formula: C24 H24 Cu2 Mo5 N6 O27 P2
• Title of publication: Solid state coordination chemistry: construction of 2D networks and 3D frameworks from phosphomolybdate clusters and binuclear Cu(ii) complexes. The syntheses and structures of [{Cu2(tpypyz)(H2O)2}(Mo5 O15)(HOPO3)2]·nH 2O [n = 2, 3; tpypyz = tetra(2-pyridyl)pyrazine]
• Authors of publication: Burkholder, Eric; Zubieta, Jon
• Journal of publication: Chemical Communications
• Year of publication: 2001
• Journal issue: 20
• Pages of publication: 2056
• a: 11.0736 ± 0.0005 Å
• b: 11.0775 ± 0.0005 Å
• c: 17.7972 ± 0.0008 Å
• α: 85.178 ± 0.001°
• β: 79.964 ± 0.001°
• γ: 68.271 ± 0.001°
• Cell volume: 1996.53 ± 0.16 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.031
• Residual factor for significantly intense reflections: 0.0259
• Weighted residual factors for significantly intense reflections: 0.0668
• Weighted residual factors for all reflections included in the refinement: 0.0687
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No