Information card for entry 7114871

Structure parameters

• Formula: C74 H82 Au3 F9 O14 P6 S3
• Calculated formula: C74 H66 Au3 F9 O14 P6 S3
• Title of publication: Observation of a P/M interconversion of a gold–phosphine helicate via   31P NMR
• Authors of publication: Schuh, Walter; Kopacka, Holger; Wurst, Klaus; Peringer, Paul
• Journal of publication: Chemical Communications
• Year of publication: 2001
• Journal issue: 21
• Pages of publication: 2186
• a: 16.8743 ± 0.0003 Å
• b: 14.8424 ± 0.0003 Å
• c: 34.0369 ± 0.0004 Å
• α: 90°
• β: 104.007 ± 0.001°
• γ: 90°
• Cell volume: 8271.2 ± 0.2 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0464
• Residual factor for significantly intense reflections: 0.0363
• Weighted residual factors for all reflections: 0.0932
• Weighted residual factors for significantly intense reflections: 0.0863
• Goodness-of-fit parameter for all reflections: 1.025
• Goodness-of-fit parameter for significantly intense reflections: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No