Information card for entry 7115006

Structure parameters

• Formula: C36 H41 Cl4.5 N5 Pd
• Calculated formula: C36 H41 Cl4.5 N5 Pd
• Title of publication: Chiral 2,6-lutidinyl-biscarbene complexes of palladium
• Authors of publication: Tulloch, Arran A. D.; Danopoulos, Andreas A.; Tizzard, Graham J.; Coles, Simon J.; Hursthouse, Michael B.; Hay-Motherwell, Robyn S.; Motherwell, William B.
• Journal of publication: Chemical Communications
• Year of publication: 2001
• Journal issue: 14
• Pages of publication: 1270
• a: 8.4782 ± 0.0004 Å
• b: 11.879 ± 0.0006 Å
• c: 20.8146 ± 0.0011 Å
• α: 75.077 ± 0.003°
• β: 83.364 ± 0.003°
• γ: 71.322 ± 0.002°
• Cell volume: 1917.65 ± 0.17 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1316
• Residual factor for significantly intense reflections: 0.0838
• Weighted residual factors for significantly intense reflections: 0.2213
• Weighted residual factors for all reflections included in the refinement: 0.2562
• Goodness-of-fit parameter for all reflections included in the refinement: 0.949
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No