Information card for entry 7115103

Structure parameters

• Chemical name: cyclo-decakis-[μ-ethanoato-bis-(-μ-ethoxy)chromium(III)]
• Formula: C60 H130 Cr10 O40
• Calculated formula: C60 H26 Cr10 O40
• Title of publication: Solvothermal synthesis of [Cr10(μ-O2CMe)10(μ-OR)20] ‘chromic wheels’ with antiferromagnetic (R = Et) and ferromagnetic (R = Me) Cr(iii)···Cr(iii) interactions
• Authors of publication: McInnes, Eric J. L.; Anson, Christopher; Powell, Annie K.; Thomson, Andrew J.; Poussereau, Sandrine; Sessoli, Roberta
• Journal of publication: Chemical Communications
• Year of publication: 2001
• Journal issue: 1
• Pages of publication: 89
• a: 9.446 ± 0.002 Å
• b: 16.052 ± 0.003 Å
• c: 28.659 ± 0.004 Å
• α: 90°
• β: 91.037 ± 0.014°
• γ: 90°
• Cell volume: 4344.8 ± 1.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.184
• Residual factor for significantly intense reflections: 0.082
• Weighted residual factors for significantly intense reflections: 0.1963
• Weighted residual factors for all reflections included in the refinement: 0.2634
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No