Information card for entry 7115202

Structure parameters

• Chemical name: [(S6-Cage-C4-OH-CH3)(tosylato)silver(I)] polymer
• Formula: C29 H49 Ag O4 S7
• Calculated formula: C29 H49 Ag O4 S7
• Title of publication: Unexpected polymeric string formation between Ag(I) and a homoleptic thioether cage: synthesis and crystal structure of [R,R′-S6tricosane] and {[Ag(R,R′-S6hexacosane)]TsO}\ιnfty
• Authors of publication: Alberto, Roger; Angst, Daniela; Schubiger, August P.; Abram, Ulrich; Ortner, Kirstin; Kaden, Thomas A.
• Journal of publication: Chemical Communications
• Year of publication: 1999
• Journal issue: 16
• Pages of publication: 1513
• a: 10.707 ± 0.004 Å
• b: 17.737 ± 0.004 Å
• c: 19.081 ± 0.008 Å
• α: 90°
• β: 103.61 ± 0.02°
• γ: 90°
• Cell volume: 3522 ± 2 ų
• Cell temperature: 208 ± 2 K
• Ambient diffraction temperature: 208 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.3067
• Residual factor for significantly intense reflections: 0.0695
• Weighted residual factors for all reflections: 0.1168
• Weighted residual factors for significantly intense reflections: 0.0671
• Goodness-of-fit parameter for all reflections: 0.918
• Goodness-of-fit parameter for significantly intense reflections: 1.078
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKa
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No