Information card for entry 7115315

Structure parameters

• Formula: C24 H40 Al2 Br2
• Calculated formula: C24 H40 Al2 Br2
• Title of publication: Synthesis, structure and reactivity of a 1-bromoalumole
• Authors of publication: Tatsuya Wasano; Tomohiro Agou; Takahiro Sasamori; Norihiro Tokitoh
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 8148
• a: 17.8044 ± 0.0001 Å
• b: 8.4388 ± 0.0001 Å
• c: 17.835 ± 0.0001 Å
• α: 90°
• β: 100.799 ± 0.0003°
• γ: 90°
• Cell volume: 2632.21 ± 0.04 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 4
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.0497
• Residual factor for significantly intense reflections: 0.0489
• Weighted residual factors for significantly intense reflections: 0.1323
• Weighted residual factors for all reflections included in the refinement: 0.1333
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.85 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No