Information card for entry 7115330

Structure parameters

• Formula: C7.5 H15 N0.75 O0.75 Zn0.75
• Calculated formula: C7.5 H15 N0.75 O0.75 Zn0.75
• Title of publication: The synthesis and structure of [Zn(TEMPO)2]2 and [Zn(mu-H)(mu^2^-mu^1^:mu^1^-TEMPO)]6
• Authors of publication: Phillip Jochmann; Douglas W. Stephan
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 8395
• a: 19.8098 ± 0.0006 Å
• b: 19.8098 ± 0.0006 Å
• c: 14.692 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 4993.1 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0313
• Residual factor for significantly intense reflections: 0.0288
• Weighted residual factors for significantly intense reflections: 0.0768
• Weighted residual factors for all reflections included in the refinement: 0.0778
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No