Information card for entry 7115477

Structure parameters

• Formula: C38.5 H52 Al N3
• Calculated formula: C38.5 H52 Al N3
• Title of publication: Yttrium-catalysed dehydrocoupling of alanes with amines
• Authors of publication: Adi E. Nako; Sarah J. Gates; Nicole Schadel; Andrew J. P. White; Mark R. Crimmin
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 9536
• a: 10.816 ± 0.0003 Å
• b: 19.4921 ± 0.0008 Å
• c: 16.6321 ± 0.0006 Å
• α: 90°
• β: 90.876 ± 0.003°
• γ: 90°
• Cell volume: 3506.1 ± 0.2 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0727
• Residual factor for significantly intense reflections: 0.0497
• Weighted residual factors for significantly intense reflections: 0.1195
• Weighted residual factors for all reflections included in the refinement: 0.1318
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No