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Information card for entry 7115585
Preview
Coordinates | 7115585.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C28 H60 N6 Na2 |
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Calculated formula | C28 H60 N6 Na2 |
SMILES | [Na]12([N](C)(C)CC[N]1(C)C)[N]1(C(C)(C)CCC=C1C)[Na]1([N](C)(C)CC[N]1(C)C)[N]12C(C)(C)CCC=C1C |
Title of publication | Dehydromethylation of alkali metal salts of the utility amide 2,2,6,6-tetramethylpiperidide (TMP) |
Authors of publication | Kennedy, Alan R.; Leenhouts, Sarah M.; Liggat, John J.; Martínez-Martínez, Antonio J.; Miller, Kimberley; Mulvey, Robert E.; O'Hara, Charles T.; O'Keefe, Philip; Steven, Alan |
Journal of publication | Chemical Communications (Cambridge, United Kingdom) |
Year of publication | 2014 |
Journal volume | 50 |
Journal issue | 73 |
Pages of publication | 10588 - 10591 |
a | 10.7005 ± 0.0003 Å |
b | 15.6464 ± 0.0005 Å |
c | 19.4063 ± 0.0007 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 3249.09 ± 0.18 Å3 |
Cell temperature | 123 ± 2 K |
Ambient diffraction temperature | 123 ± 2 K |
Number of distinct elements | 4 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0705 |
Residual factor for significantly intense reflections | 0.0527 |
Weighted residual factors for significantly intense reflections | 0.1453 |
Weighted residual factors for all reflections included in the refinement | 0.156 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.079 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7115585.html
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