Information card for entry 7115639

Structure parameters

• Common name: 4
• Chemical name: 4
• Formula: C32 H32 F6 N2 O4 P2 Ru
• Calculated formula: C32 H32 F6 N2 O4 P2 Ru
• Title of publication: Hydrogenation of amides catalyzed by a combined catalytic system of a Ru complex with a zinc salt
• Authors of publication: Yusuke Kita; Takafumi Higuchi; Kazushi Mashima
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 11211
• a: 12.66 ± 0.018 Å
• b: 13.268 ± 0.019 Å
• c: 13.386 ± 0.018 Å
• α: 119.526 ± 0.001°
• β: 92.516 ± 0.015°
• γ: 115.846 ± 0.008°
• Cell volume: 1662 ± 4 ų
• Cell temperature: 113 ± 2 K
• Ambient diffraction temperature: 113 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1648
• Residual factor for significantly intense reflections: 0.1234
• Weighted residual factors for significantly intense reflections: 0.306
• Weighted residual factors for all reflections included in the refinement: 0.3475
• Goodness-of-fit parameter for all reflections included in the refinement: 1.131
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No