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Information card for entry 7115766
Preview
Coordinates | 7115766.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C21 H37 F N O6 P Si2 W |
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Calculated formula | C21 H37 F N O6 P Si2 W |
SMILES | C([P](F)(ON1C(CCCC1(C)C)(C)C)[W](C#[O])(C#[O])(C#[O])(C#[O])C#[O])([Si](C)(C)C)[Si](C)(C)C |
Title of publication | Selective phosphanyl complex trapping using TEMPO. Synthesis and reactivity of P-functional P-nitroxyl phosphane complexes |
Authors of publication | Vitaly Nesterov; Zheng-Wang Qu; Gregor Schnakenburg; Stefan Grimme; Rainer Streubel |
Journal of publication | Chem.Commun. |
Year of publication | 2014 |
Journal volume | 50 |
Pages of publication | 12508 |
a | 13.1797 ± 0.0003 Å |
b | 14.2791 ± 0.0003 Å |
c | 15.1502 ± 0.0003 Å |
α | 96.4947 ± 0.0011° |
β | 90.2543 ± 0.0011° |
γ | 93.9588 ± 0.0011° |
Cell volume | 2825.91 ± 0.1 Å3 |
Cell temperature | 123 ± 2 K |
Ambient diffraction temperature | 123 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.029 |
Residual factor for significantly intense reflections | 0.0235 |
Weighted residual factors for significantly intense reflections | 0.0557 |
Weighted residual factors for all reflections included in the refinement | 0.0574 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.002 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7115766.html
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