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Information card for entry 7115778
Preview
Coordinates | 7115778.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C48 H42 Si |
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Calculated formula | C48 H42 Si |
SMILES | [Si](c1c(cccc1c1c(cc(cc1C)C)C)c1c(cc(cc1C)C)C)(/C=C\c1ccccc1)(C#Cc1ccccc1)C#Cc1ccccc1 |
Title of publication | A facile access to a novel NHC-stabilized silyliumylidene ion and C-H activation of phenylacetylene |
Authors of publication | Syed Usman Ahmad; Tibor Szilvasi; Shigeyoshi Inoue |
Journal of publication | Chem.Commun. |
Year of publication | 2014 |
Journal volume | 50 |
Pages of publication | 12619 |
a | 26.3057 ± 0.0003 Å |
b | 8.3377 ± 0.0001 Å |
c | 34.2192 ± 0.0004 Å |
α | 90° |
β | 99.146 ± 0.001° |
γ | 90° |
Cell volume | 7409.85 ± 0.15 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 0.1 K |
Number of distinct elements | 3 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.047 |
Residual factor for significantly intense reflections | 0.0414 |
Weighted residual factors for significantly intense reflections | 0.1147 |
Weighted residual factors for all reflections included in the refinement | 0.1203 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.026 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7115778.html
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