Information card for entry 7115838

Structure parameters

• Formula: C69 H77 B Cr F21 N2 Si2
• Calculated formula: C69 H77 B Cr F21 N2 Si2
• Title of publication: A bis(amido) ligand set that supports two-coordinate chromium in the +1, +2, and +3 oxidation states
• Authors of publication: Irene C. Cai; Michael I. Lipschutz; T. Don Tilley
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 13062
• a: 13.4838 ± 0.0008 Å
• b: 15.8748 ± 0.0009 Å
• c: 18.4544 ± 0.001 Å
• α: 67.15 ± 0.003°
• β: 89.637 ± 0.003°
• γ: 69.398 ± 0.003°
• Cell volume: 3368.3 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.06
• Residual factor for significantly intense reflections: 0.0494
• Weighted residual factors for significantly intense reflections: 0.1204
• Weighted residual factors for all reflections included in the refinement: 0.1282
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No