Information card for entry 7115947

Structure parameters

• Formula: C20 H8 O8 Pb2
• Calculated formula: C20 H8 O8 Pb2
• Title of publication: A facile single crystal to single crystal transition with significant structural contraction on desolvation
• Authors of publication: Jane V. Knichal; William J. Gee; Andrew D. Burrows; Paul R. Raithby; Simon J. Teat; Chick C. Wilson
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 14436
• a: 9.379 ± 0.0004 Å
• b: 10.013 ± 0.0003 Å
• c: 10.318 ± 0.0004 Å
• α: 100.148 ± 0.003°
• β: 91.407 ± 0.003°
• γ: 107.941 ± 0.003°
• Cell volume: 904.22 ± 0.06 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0987
• Residual factor for significantly intense reflections: 0.0505
• Weighted residual factors for significantly intense reflections: 0.1064
• Weighted residual factors for all reflections included in the refinement: 0.1203
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.7749 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No