Information card for entry 7116154

Structure parameters

• Chemical name: 1,3,5,7-tetrakis[bis(trimethylsilyl)methyl]-9,9,10,10-tetramethyl-2,4,6,8-tetraoxa-1,3,5,7-tetrastannaadamantane + tetrakis[bis(trimethylsilyl)methyl]-bis-1,3-2,4-μ-(iso-propyliden)-bis-1,2-3,4-μ-oxo-tetrastannahedrane
• Formula: C34 H88 O3 Si8 Sn4
• Calculated formula: C34 H88 O3 Si8 Sn4
• Title of publication: [Me2C{SnCH(SiMe3)2}2]2. A mu-Me2C-bridged tetrastanna tetrahedrane
• Authors of publication: Michael Wagner; Michael Lutter; Bernhard Zobel; Wolf Hiller; Marc H. Prosenc; Klaus Jurkschat
• Journal of publication: Chem.Commun.
• Year of publication: 2015
• Journal volume: 51
• Pages of publication: 153
• a: 27.325 ± 0.0011 Å
• b: 13.2488 ± 0.0004 Å
• c: 16.5435 ± 0.0005 Å
• α: 90°
• β: 109.718 ± 0.004°
• γ: 90°
• Cell volume: 5638 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0357
• Residual factor for significantly intense reflections: 0.0272
• Weighted residual factors for significantly intense reflections: 0.0561
• Weighted residual factors for all reflections included in the refinement: 0.0581
• Goodness-of-fit parameter for all reflections included in the refinement: 1.202
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No