Information card for entry 7116206

Structure parameters

• Formula: C44 H47 B2 F8 N7 O3
• Calculated formula: C44 H47 B2 F8 N7 O3
• Title of publication: Controlled access to a heterometallic N-heterocyclic carbene helicate.
• Authors of publication: Teng, Qiaoqiao; Huynh, Han Vinh
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2014
• Journal volume: 51
• Journal issue: 7
• Pages of publication: 1248 - 1251
• a: 8.6769 ± 0.0011 Å
• b: 15.92 ± 0.002 Å
• c: 17.935 ± 0.003 Å
• α: 115.794 ± 0.004°
• β: 103.951 ± 0.003°
• γ: 90.302 ± 0.003°
• Cell volume: 2147.6 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1026
• Residual factor for significantly intense reflections: 0.072
• Weighted residual factors for significantly intense reflections: 0.1545
• Weighted residual factors for all reflections included in the refinement: 0.1672
• Goodness-of-fit parameter for all reflections included in the refinement: 1.09
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No