Information card for entry 7116211

Structure parameters

• Common name: tetramethylammonium tetradecaniobophosphate
• Formula: C28 H84 N7 Nb14 O68 P
• Calculated formula: C28 H84 N7 Nb14 O68.1495 P
• Title of publication: Reversible capping/uncapping of phosphorous-centered Keggin-type polyoxoniobate clusters.
• Authors of publication: Son, Jung-Ho; Casey, William H.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2015
• Journal volume: 51
• Journal issue: 8
• Pages of publication: 1436 - 1438
• a: 13.429 ± 0.007 Å
• b: 14.943 ± 0.008 Å
• c: 25.521 ± 0.013 Å
• α: 77.02 ± 0.007°
• β: 88.45 ± 0.007°
• γ: 82.922 ± 0.007°
• Cell volume: 4952 ± 4 ų
• Cell temperature: 88 ± 2 K
• Ambient diffraction temperature: 88 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1169
• Residual factor for significantly intense reflections: 0.0877
• Weighted residual factors for significantly intense reflections: 0.2135
• Weighted residual factors for all reflections included in the refinement: 0.2301
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No