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Information card for entry 7116273
Preview
Coordinates | 7116273.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C23 H16 F6 I2 O7 S2 |
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Calculated formula | C23 H16 F6 I2 O7 S2 |
Title of publication | Formation and in situ reactions of hypervalent iodonium alkynyl triflates to form cyanocarbenes. |
Authors of publication | Dempsey Hyatt, I. F.; Nasrallah, Daniel J.; Maxwell, Michael A.; Hairston, A Christina F; Abdalhameed, Manahil M.; Croatt, Mitchell P. |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2015 |
Journal volume | 51 |
Journal issue | 25 |
Pages of publication | 5287 - 5289 |
a | 10.5549 ± 0.0009 Å |
b | 13.6694 ± 0.0012 Å |
c | 19.151 ± 0.0016 Å |
α | 90° |
β | 94.31 ± 0.001° |
γ | 90° |
Cell volume | 2755.3 ± 0.4 Å3 |
Cell temperature | 193 ± 2 K |
Ambient diffraction temperature | 193 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0664 |
Residual factor for significantly intense reflections | 0.0552 |
Weighted residual factors for significantly intense reflections | 0.1399 |
Weighted residual factors for all reflections included in the refinement | 0.1483 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.108 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7116273.html
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