Crystallography Open Database

Information card for entry 7116286

Preview

Coordinates	7116286.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H24 Cl3 N O2 Si
Calculated formula	C26 H24 Cl3 N O2 Si
Title of publication	Multi-site cyclization via initial C-H activation using a rhodium(iii) catalyst: rapid assembly of frameworks containing indoles and indolines.
Authors of publication	Huang, Ji-Rong; Qin, Liu; Zhu, Yu-Qin; Song, Qiang; Dong, Lin
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2015
Journal volume	51
Journal issue	14
Pages of publication	2844
a	9.6847 ± 0.0007 Å
b	10.6101 ± 0.0008 Å
c	12.7428 ± 0.001 Å
α	82.268 ± 0.006°
β	87.114 ± 0.006°
γ	75.081 ± 0.007°
Cell volume	1253.58 ± 0.17 Å³
Cell temperature	170 ± 2 K
Ambient diffraction temperature	170 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.077
Residual factor for significantly intense reflections	0.0556
Weighted residual factors for significantly intense reflections	0.1246
Weighted residual factors for all reflections included in the refinement	0.1426
Goodness-of-fit parameter for all reflections included in the refinement	1.022
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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