Information card for entry 7116409

Structure parameters

• Formula: C149 H248 B8 P8 Sn4
• Calculated formula: C149 H248 B8 P8 Sn4
• Title of publication: Impact of a rigid backbone on the structure of an agostically-stabilised dialkylstannylene: isolation of an unusual bridged stannyl-stannylene
• Authors of publication: Keith Izod; Casey M. Dixon; Ross W. Harrington; Michael R. Probert
• Journal of publication: Chem.Commun.
• Year of publication: 2015
• Journal volume: 51
• Pages of publication: 679
• a: 14.0885 ± 0.0001 Å
• b: 26.577 ± 0.0002 Å
• c: 20.0509 ± 0.0002 Å
• α: 90°
• β: 95.273 ± 0.001°
• γ: 90°
• Cell volume: 7475.89 ± 0.11 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0389
• Residual factor for significantly intense reflections: 0.0278
• Weighted residual factors for significantly intense reflections: 0.0558
• Weighted residual factors for all reflections included in the refinement: 0.0604
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No