Information card for entry 7116528

Structure parameters

• Formula: C16 H111 Cu4 Dy2 K2 N16 O101.5 Si2 W22
• Calculated formula: C16 H64 Cu4 Dy2 K2 N16 O99.5 Si2 W22
• Title of publication: Polyoxometalates-based heterometallic organic-inorganic hybrid materials for rapid adsorption and selective separation of methylene blue from aqueous solutions
• Authors of publication: Fei-Yan Yi; Wei Zhu; Song Dang; Jian-Ping Li; Dai Wu; Yun-hui Li; Zhong-Ming Sun
• Journal of publication: Chem.Commun.
• Year of publication: 2015
• Journal volume: 51
• Pages of publication: 3336
• a: 20.5847 ± 0.0011 Å
• b: 13.4613 ± 0.0007 Å
• c: 22.9069 ± 0.0013 Å
• α: 90°
• β: 101.973 ± 0.001°
• γ: 90°
• Cell volume: 6209.3 ± 0.6 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 9
• Space group number: 8
• Hermann-Mauguin space group symbol: C 1 m 1
• Hall space group symbol: C -2y
• Residual factor for all reflections: 0.0497
• Residual factor for significantly intense reflections: 0.0407
• Weighted residual factors for significantly intense reflections: 0.097
• Weighted residual factors for all reflections included in the refinement: 0.1028
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No