Information card for entry 7116662

Structure parameters

• Formula: C70 H110 Li2 O2 Pb2 Si4
• Calculated formula: C70 H110 Li2 O2 Pb2 Si4
• Title of publication: A reversible two-electron redox system involving a divalent lead species
• Authors of publication: Masaichi Saito; Marisa Nakada; Takuya Kuwabara; Mao Minoura
• Journal of publication: Chem.Commun.
• Year of publication: 2015
• Journal volume: 51
• Pages of publication: 4674
• a: 12.2658 ± 0.001 Å
• b: 16.7325 ± 0.0013 Å
• c: 20.375 ± 0.0016 Å
• α: 99.254 ± 0.001°
• β: 107.15 ± 0.001°
• γ: 107.882 ± 0.001°
• Cell volume: 3654.6 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0444
• Residual factor for significantly intense reflections: 0.0301
• Weighted residual factors for significantly intense reflections: 0.0675
• Weighted residual factors for all reflections included in the refinement: 0.0738
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No