Information card for entry 7116936

Structure parameters

• Formula: C30.3 H25.6 Cl0.6 N4 O2 Rh
• Calculated formula: C30.3 H25.6 Cl0.6 N4 O2 Rh
• Title of publication: Rh/Cu-catalyzed multiple C-H, C-C, and C-N bond cleavage: facile synthesis of pyrido[2,1-a]indoles from 1-(pyridin-2-yl)-1H-indoles and gamma-substituted propargyl alcohols
• Authors of publication: Ting Li; Zhen Wang; Mingliang Zhang; Hui-Jun Zhang; Ting-Bin Wen
• Journal of publication: Chem.Commun.
• Year of publication: 2015
• Journal volume: 51
• Pages of publication: 6777
• a: 9.6401 ± 0.0019 Å
• b: 11.069 ± 0.002 Å
• c: 12.562 ± 0.003 Å
• α: 82.69 ± 0.03°
• β: 77.98 ± 0.03°
• γ: 83.72 ± 0.03°
• Cell volume: 1295.6 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0727
• Residual factor for significantly intense reflections: 0.0505
• Weighted residual factors for significantly intense reflections: 0.1225
• Weighted residual factors for all reflections included in the refinement: 0.1693
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No