Information card for entry 7117175

Structure parameters

• Chemical name: 2,17-Dioxo[3,3](4,4')biphenylophane
• Formula: C30 H24 O2
• Calculated formula: C30 H24 O2
• Title of publication: One-step synthesis of a cyclic 2,17-dioxo[3,3](4,4') biphenylophane and first preparation of a microporous polymer network from a macrocyclic precursor by cyclotrimerization
• Authors of publication: Suman Kalyan Samanta; Eduard Preis; Christian W. Lehmann; Richard Goddard; Saientan Bag; Prabal K. Maiti; Gunther Brunklaus; Ullrich Scherf
• Journal of publication: Chem.Commun.
• Year of publication: 2015
• Journal volume: 51
• Pages of publication: 9046
• a: 31.067 ± 0.015 Å
• b: 13.835 ± 0.006 Å
• c: 15.67 ± 0.007 Å
• α: 90°
• β: 93.254 ± 0.011°
• γ: 90°
• Cell volume: 6724 ± 5 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 3
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1448
• Residual factor for significantly intense reflections: 0.0858
• Weighted residual factors for significantly intense reflections: 0.1739
• Weighted residual factors for all reflections included in the refinement: 0.1979
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.8 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No