Information card for entry 7117243

Structure parameters

• Formula: C32 H41 Cl2 N3 Pd
• Calculated formula: C32 H41 Cl2 N3 Pd
• Title of publication: Two-step solid-state synthesis of PEPPSI-type compounds
• Authors of publication: Christopher J. Adams; Matteo Lusi; Emily M. Mutambi; A. Guy Orpen
• Journal of publication: Chem.Commun.
• Year of publication: 2015
• Journal volume: 51
• Pages of publication: 9632
• a: 9.7411 ± 0.0005 Å
• b: 22.3057 ± 0.001 Å
• c: 14.8046 ± 0.0008 Å
• α: 90°
• β: 98.163 ± 0.003°
• γ: 90°
• Cell volume: 3184.2 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0634
• Residual factor for significantly intense reflections: 0.037
• Weighted residual factors for significantly intense reflections: 0.0877
• Weighted residual factors for all reflections included in the refinement: 0.1033
• Goodness-of-fit parameter for all reflections included in the refinement: 0.968
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No