Information card for entry 7117429

Structure parameters

• Formula: C48 H50 Bi Cl2 N2 Sb
• Calculated formula: C48 H50 Bi Cl2 N2 Sb
• Title of publication: Accessing heavy allyl-analogous [(TerN)2E]- (E = Sb, Bi) ions and their reactivity towards ECl3
• Authors of publication: Alexander Hinz; Axel Schulz; Alexander Villinger
• Journal of publication: Chem.Commun.
• Year of publication: 2015
• Journal volume: 51
• Pages of publication: 11437
• a: 14.6206 ± 0.0012 Å
• b: 15.5222 ± 0.0012 Å
• c: 18.7038 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4244.7 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0728
• Residual factor for significantly intense reflections: 0.0342
• Weighted residual factors for significantly intense reflections: 0.0596
• Weighted residual factors for all reflections included in the refinement: 0.0692
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No