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Information card for entry 7117448
Preview
Coordinates | 7117448.cif |
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Original paper (by DOI) | HTML |
Formula | C30 H49 N O Si2 |
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Calculated formula | C30 H49 N O Si2 |
Title of publication | Ni(ii)-catalyzed dehydrative alkynylation of unactivated (hetero)aryl C-H bonds using oxygen: a user-friendly approach. |
Authors of publication | Liu, Yan-Hua; Liu, Yue-Jin; Yan, Sheng-Yi; Shi, Bing-Feng |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2015 |
Journal volume | 51 |
Journal issue | 58 |
Pages of publication | 11650 - 11653 |
a | 12.502 ± 0.0008 Å |
b | 15.8137 ± 0.0009 Å |
c | 17.4136 ± 0.001 Å |
α | 74.497 ± 0.002° |
β | 75.487 ± 0.001° |
γ | 76.75 ± 0.002° |
Cell volume | 3162.7 ± 0.3 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.2309 |
Residual factor for significantly intense reflections | 0.1479 |
Weighted residual factors for significantly intense reflections | 0.3813 |
Weighted residual factors for all reflections included in the refinement | 0.441 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.191 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7117448.html
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