Information card for entry 7117588

Structure parameters

• Formula: C71 H58 F6 N2 O7 P S2
• Calculated formula: C71 H58.0001 F6 N2 O7 P S2
• Title of publication: Isolation of a Lewis base stabilized parent phosphenium (PH2(+)) and related species.
• Authors of publication: Liu, Liu; Ruiz, David A.; Dahcheh, Fatme; Bertrand, Guy
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2015
• Journal volume: 51
• Journal issue: 64
• Pages of publication: 12732 - 12735
• a: 14.4808 ± 0.0011 Å
• b: 14.6435 ± 0.0011 Å
• c: 15.4095 ± 0.001 Å
• α: 83.039 ± 0.002°
• β: 84.164 ± 0.002°
• γ: 77.715 ± 0.002°
• Cell volume: 3159.5 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0635
• Residual factor for significantly intense reflections: 0.0527
• Weighted residual factors for significantly intense reflections: 0.1182
• Weighted residual factors for all reflections included in the refinement: 0.1251
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No