Information card for entry 7117590

Structure parameters

• Formula: C69 H57 Au2 Cl2 N2 P
• Calculated formula: C69 H57 Au2.0001 Cl2.0001 N2 P
• Title of publication: Isolation of a Lewis base stabilized parent phosphenium (PH2(+)) and related species.
• Authors of publication: Liu, Liu; Ruiz, David A.; Dahcheh, Fatme; Bertrand, Guy
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2015
• Journal volume: 51
• Journal issue: 64
• Pages of publication: 12732 - 12735
• a: 15.4817 ± 0.0009 Å
• b: 18.0766 ± 0.001 Å
• c: 24.4404 ± 0.0014 Å
• α: 90°
• β: 98.019 ± 0.002°
• γ: 90°
• Cell volume: 6772.9 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0492
• Residual factor for significantly intense reflections: 0.0447
• Weighted residual factors for significantly intense reflections: 0.1217
• Weighted residual factors for all reflections included in the refinement: 0.1246
• Goodness-of-fit parameter for all reflections included in the refinement: 1.106
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No