Information card for entry 7117640

Structure parameters

• Formula: C11 H17 N O5 Pb
• Calculated formula: C11 H17 N O5 Pb
• Title of publication: Pb3[C6(CH3)3(CO2)3H6]2[DMF]3: first layered Pb-Kemp's triacid complex
• Authors of publication: Saet Byeol Kim; Dong Woo Lee; Suk-Kyu Chang; Kang Min Ok
• Journal of publication: Chem.Commun.
• Year of publication: 2015
• Journal volume: 51
• Pages of publication: 13166
• a: 14.4445 ± 0.0006 Å
• b: 14.4445 ± 0.0006 Å
• c: 34.0453 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 6151.7 ± 0.4 ų
• Cell temperature: 173 ± 0.2 K
• Ambient diffraction temperature: 173 ± 0.2 K
• Number of distinct elements: 5
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.1398
• Residual factor for significantly intense reflections: 0.0465
• Weighted residual factors for significantly intense reflections: 0.0625
• Weighted residual factors for all reflections included in the refinement: 0.0778
• Goodness-of-fit parameter for all reflections included in the refinement: 0.771
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No