Information card for entry 7117662

Structure parameters

• Formula: C22 H24 Cl5 Cu Mn4 P4
• Calculated formula: C22 H24 Cl5 Cu Mn4 P4
• Title of publication: The synthesis of the heterocubane cluster [{CpMn}4(mu3-P)4] as a tetrahedral shaped starting material for the formation of polymeric coordination compounds
• Authors of publication: Sebastian Heinl; Konrad Kiefer; Gabor Balazs; Claudia Wickleder; Manfred Scheer
• Journal of publication: Chem.Commun.
• Year of publication: 2015
• Journal volume: 51
• Pages of publication: 13474
• a: 23.8316 ± 0.0006 Å
• b: 12.8659 ± 0.0003 Å
• c: 18.4127 ± 0.0004 Å
• α: 90°
• β: 93.404 ± 0.002°
• γ: 90°
• Cell volume: 5635.6 ± 0.2 ų
• Cell temperature: 123 ± 0.4 K
• Ambient diffraction temperature: 123 ± 0.4 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0451
• Residual factor for significantly intense reflections: 0.0414
• Weighted residual factors for significantly intense reflections: 0.1276
• Weighted residual factors for all reflections included in the refinement: 0.1294
• Goodness-of-fit parameter for all reflections included in the refinement: 1.096
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No