Information card for entry 7118193

Structure parameters

• Formula: C29 H24 F9 O9 P2 S3 Sb
• Calculated formula: C29 H24 F9 O9 P2 S3 Sb
• Title of publication: Distinction between coordination and phosphine ligand oxidation: interactions of di- and triphosphines with Pn^3+^ (Pn = P, As, Sb, Bi)
• Authors of publication: Chitnis, Saurabh S.; Vos, Kevin A.; Burford, Neil; McDonald, Robert; Ferguson, Michael J.
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2016
• Journal volume: 52
• Pages of publication: 685 - 688
• a: 13.3718 ± 0.0004 Å
• b: 17.5496 ± 0.0006 Å
• c: 15.4871 ± 0.0005 Å
• α: 90°
• β: 102.96 ± 0.0015°
• γ: 90°
• Cell volume: 3541.8 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0481
• Residual factor for significantly intense reflections: 0.0416
• Weighted residual factors for significantly intense reflections: 0.1055
• Weighted residual factors for all reflections included in the refinement: 0.1119
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No