Information card for entry 7118342

Structure parameters

• Formula: C42 H58 N2 O4.5 P Si
• Calculated formula: C42 H58 N2 O4.5 P Si
• Title of publication: Carbamoyl anion-initiated cascade reaction for stereoselective synthesis of substituted α-hydroxy-β-amino amides.
• Authors of publication: Lin, Chao-Yang; Ma, Peng-Ju; Sun, Zhao; Lu, Chong-Dao; Xu, Yan-Jun
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 5
• Pages of publication: 912 - 915
• a: 11.473 ± 0.004 Å
• b: 13.299 ± 0.005 Å
• c: 13.766 ± 0.005 Å
• α: 85.201 ± 0.005°
• β: 86.909 ± 0.005°
• γ: 86.437 ± 0.005°
• Cell volume: 2086.5 ± 1.3 ų
• Cell temperature: 296.15 K
• Ambient diffraction temperature: 296.15 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1755
• Residual factor for significantly intense reflections: 0.075
• Weighted residual factors for significantly intense reflections: 0.1911
• Weighted residual factors for all reflections included in the refinement: 0.2528
• Goodness-of-fit parameter for all reflections included in the refinement: 0.911
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No