Information card for entry 7118412

Structure parameters

• Formula: C35 H48 F3 Ge N3 O3 S
• Calculated formula: C35 H48 F3 Ge N3 O3 S
• Title of publication: Synthesis, characterization, and electronic structures of a methyl germyliumylidene ion and germylone-group VI metal complexes
• Authors of publication: Bochao Su; Rakesh Ganguly; Yongxin Li; Rei Kinjo
• Journal of publication: Chem.Commun.
• Year of publication: 2016
• Journal volume: 52
• Pages of publication: 613
• a: 11.7454 ± 0.0009 Å
• b: 24.4796 ± 0.0019 Å
• c: 13.3037 ± 0.001 Å
• α: 90°
• β: 115.166 ± 0.002°
• γ: 90°
• Cell volume: 3462 ± 0.5 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0726
• Residual factor for significantly intense reflections: 0.0482
• Weighted residual factors for significantly intense reflections: 0.1075
• Weighted residual factors for all reflections included in the refinement: 0.1184
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No