Information card for entry 7118429

Structure parameters

• Formula: C18 H32 N O6 Si
• Calculated formula: C18 H32 N O6 Si
• SMILES: [Si](O[C@@H]1[C@H](O[C@@H]2[C@H]1N(C(=O)OC(C)(C)C)C(=O)C2)CO)(C(C)(C)C)(C)C
• Title of publication: The asymmetric total synthesis of (+)-N-acetyl norloline
• Authors of publication: Jian-Liang Ye; Yang Liu; Zhi-Ping Yang; Pei-Qiang Huang
• Journal of publication: Chem.Commun.
• Year of publication: 2016
• Journal volume: 52
• Pages of publication: 561
• a: 6.826 ± 0.0015 Å
• b: 9.791 ± 0.002 Å
• c: 30.82 ± 0.007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2059.8 ± 0.8 ų
• Cell temperature: 273.15 K
• Ambient diffraction temperature: 273.15 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0522
• Residual factor for significantly intense reflections: 0.0464
• Weighted residual factors for significantly intense reflections: 0.1214
• Weighted residual factors for all reflections included in the refinement: 0.1251
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0367
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No