Information card for entry 7118472

Structure parameters

• Formula: C30 H25 F9 N O9 P2 S3 Sb
• Calculated formula: C30 H25 F9 N O9 P2 S3 Sb
• SMILES: [Sb]1(P(CP1(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)(OS(=O)(=O)C(F)(F)F)(OS(=O)(=O)C(F)(F)F)OS(=O)(=O)C(F)(F)F.N#CC
• Title of publication: Distinction between coordination and phosphine ligand oxidation: interactions of di- and triphosphines with Pn^3+^ (Pn = P, As, Sb, Bi)
• Authors of publication: Chitnis, Saurabh S.; Vos, Kevin A.; Burford, Neil; McDonald, Robert; Ferguson, Michael J.
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2016
• Journal volume: 52
• Pages of publication: 685 - 688
• a: 9.1263 ± 0.0005 Å
• b: 19.3196 ± 0.001 Å
• c: 21.6426 ± 0.0011 Å
• α: 90°
• β: 99.3749 ± 0.0006°
• γ: 90°
• Cell volume: 3765 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0282
• Residual factor for significantly intense reflections: 0.0233
• Weighted residual factors for significantly intense reflections: 0.0543
• Weighted residual factors for all reflections included in the refinement: 0.0568
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7118192
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No