Information card for entry 7118847

Structure parameters

• Formula: C21 H31 B2 F2 O3 P
• Calculated formula: C21 H31 B2 F2 O3 P
• Title of publication: New outcomes of Lewis base addition to diboranes(4): electronic effects override strong steric disincentives.
• Authors of publication: Arnold, Nicole; Braunschweig, Holger; Damme, Alexander; Dewhurst, Rian D.; Pentecost, Leanne; Radacki, Krzysztof; Stellwag-Konertz, Sascha; Thiess, Torsten; Trumpp, Alexandra; Vargas, Alfredo
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 27
• Pages of publication: 4898 - 4901
• a: 10.3 ± 0.006 Å
• b: 14.375 ± 0.01 Å
• c: 15.204 ± 0.009 Å
• α: 90°
• β: 104.85 ± 0.014°
• γ: 90°
• Cell volume: 2176 ± 2 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0758
• Residual factor for significantly intense reflections: 0.0545
• Weighted residual factors for significantly intense reflections: 0.1343
• Weighted residual factors for all reflections included in the refinement: 0.1455
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No