Information card for entry 7119051

Structure parameters

• Chemical name: complex 2
• Formula: C58.5 H79 Cl8 N5 W
• Calculated formula: C58.5 H79 Cl8 N5 W
• Title of publication: Application of imidazolinium salts and N-heterocyclic olefins for the synthesis of anionic and neutral tungsten imido alkylidene complexes
• Authors of publication: Dominik A. Imbrich; Wolfgang Frey; Stefan Naumann; Michael R. Buchmeiser
• Journal of publication: Chem.Commun.
• Year of publication: 2016
• Journal volume: 52
• Pages of publication: 6099
• a: 21.6865 ± 0.0019 Å
• b: 18.8737 ± 0.0016 Å
• c: 16.1005 ± 0.0013 Å
• α: 90°
• β: 106.667 ± 0.003°
• γ: 90°
• Cell volume: 6313.1 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.08
• Residual factor for significantly intense reflections: 0.0566
• Weighted residual factors for significantly intense reflections: 0.1458
• Weighted residual factors for all reflections included in the refinement: 0.1608
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No