Information card for entry 7119279

Structure parameters

• Formula: C255 H280 La4 N20 O4 Si8
• Calculated formula: C255 H279 La4 N20 O4 Si8
• Title of publication: Bis(amidinate) ligands in early lanthanide chemistry - synthesis, structures, and hydroamination catalysis.
• Authors of publication: Kazeminejad, Neda; Munzel, Denise; Gamer, Michael T.; Roesky, Peter W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2017
• Journal volume: 53
• Journal issue: 6
• Pages of publication: 1060 - 1063
• a: 20.8963 ± 0.0009 Å
• b: 22.8615 ± 0.0008 Å
• c: 25.1772 ± 0.001 Å
• α: 90°
• β: 94.338 ± 0.003°
• γ: 90°
• Cell volume: 11993.2 ± 0.8 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.2382
• Residual factor for significantly intense reflections: 0.1308
• Weighted residual factors for significantly intense reflections: 0.281
• Weighted residual factors for all reflections included in the refinement: 0.3663
• Goodness-of-fit parameter for all reflections included in the refinement: 1.103
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No