Crystallography Open Database

Information card for entry 7119519

7119518 << 7119519 >> 7119520

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Coordinates	7119519.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Mo5V1
Formula	C48 H107 Mo5 N3 O19 V
Calculated formula	C48 H107 Mo4.882 N3 O19 V1.118
Title of publication	[V4Mo3O14(NAr)3(μ2-NAr)3](2-): the first polyarylimido-stabilized molybdovanadate cluster.
Authors of publication	Huang, Yichao; Zhang, Jiangwei; Ge, Jingxuan; Sui, Chong; Hao, Jian; Wei, Yongge
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2017
Journal volume	53
Journal issue	17
Pages of publication	2551 - 2554
a	29.2304 ± 0.0018 Å
b	18.5275 ± 0.001 Å
c	27.1217 ± 0.0013 Å
α	90°
β	113.089 ± 0.007°
γ	90°
Cell volume	13511.6 ± 1.5 Å³
Cell temperature	102.8 K
Ambient diffraction temperature	102.8 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1266
Residual factor for significantly intense reflections	0.0692
Weighted residual factors for significantly intense reflections	0.1556
Weighted residual factors for all reflections included in the refinement	0.1933
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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