Information card for entry 7119715

Structure parameters

• Formula: C33 H47 N3 O Pb
• Calculated formula: C33 H47 N3 O Pb
• Title of publication: Reactivity of heavy carbene analogues towards oxidants: a redox active ligand-enabled isolation of a paramagnetic stannylene.
• Authors of publication: Janes, Trevor; Zatsepin, Pavel; Song, Datong
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2017
• Journal volume: 53
• Journal issue: 21
• Pages of publication: 3090 - 3093
• a: 14.8076 ± 0.0012 Å
• b: 26.177 ± 0.002 Å
• c: 20.3861 ± 0.0017 Å
• α: 90°
• β: 92.81 ± 0.004°
• γ: 90°
• Cell volume: 7892.5 ± 1.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.159
• Residual factor for significantly intense reflections: 0.0663
• Weighted residual factors for significantly intense reflections: 0.1341
• Weighted residual factors for all reflections included in the refinement: 0.1673
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No