Information card for entry 7120259

Structure parameters

• Formula: C116 Ag2 Cr Lu2 Mn4 N14 O78 Si2 W18
• Calculated formula: C116 Ag2 Cr Lu2 Mn4 N14 O78 Si2 W18
• Title of publication: A modular synthesis approach to multinuclear heterometallic oxo clusters in polyoxometalates
• Authors of publication: Minato, Takuo; Suzuki, Kosuke; Ohata, Yusuke; Yamaguchi, Kazuya; Mizuno, Noritaka
• Journal of publication: Chem. Commun.
• Year of publication: 2017
• a: 17.4607 ± 0.0003 Å
• b: 18.5296 ± 0.0006 Å
• c: 19.3013 ± 0.0003 Å
• α: 61.295 ± 0.001°
• β: 63.252 ± 0.001°
• γ: 82.415 ± 0.001°
• Cell volume: 4862.9 ± 0.2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.062
• Residual factor for significantly intense reflections: 0.0506
• Weighted residual factors for significantly intense reflections: 0.1351
• Weighted residual factors for all reflections included in the refinement: 0.142
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No