Information card for entry 7120319

Structure parameters

• Formula: C50 H66 Cl Ga N2 P
• Calculated formula: C50 H66 Cl Ga N2 P
• Title of publication: An NHC‒phosphinidenyl as a synthon for new group 13/15 compounds
• Authors of publication: Lemp, Otfried; Balmer, Markus; Reiter, Kevin; Weigend, Florian; von Hänisch, Carsten
• Journal of publication: Chem. Commun.
• Year of publication: 2017
• a: 10.8193 ± 0.0005 Å
• b: 13.6219 ± 0.0007 Å
• c: 17.1442 ± 0.0008 Å
• α: 105.261 ± 0.002°
• β: 101.977 ± 0.002°
• γ: 98.128 ± 0.002°
• Cell volume: 2332.5 ± 0.2 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 109.99 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0553
• Residual factor for significantly intense reflections: 0.0366
• Weighted residual factors for significantly intense reflections: 0.0733
• Weighted residual factors for all reflections included in the refinement: 0.0795
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No